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Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
181
STUDY ON THE INFLUENCE OF FIBER ORIENTATION ON PALF
REINFORCED BISPHENOL COMPOSITES
Vinod B1
, Dr. Sudev L J2
1
Asst Professor, Department of Mechanical Engg, VVCE, Mysore, India
2
Professor, Department of Mechanical Engg, VVCE, Mysore, India
ABSTRACT
The main advantage of a composite material over conventional material like a monolithic metal is the
combination of different properties which are seldom found in the conventional material. In recent years natural fibers
appear to be the outstanding materials which come as the viable and abundant substitute for the expensive and
nonrenewable synthetic fiber. Pineapple leaf fiber (PALF) is one of them that have also good potential as reinforcement
in thermoset composite. The objective of the present work is to investigate the effect of fiber orientation on the
mechanical properties of PALF reinforced Bisphenol composite and explores the potential of using PALF as reinforcing
material. In this paper the mechanical properties like tensile, flexural and impact behavior are studied. From this
experimental study, it was observed that the fiber orientation greatly influences the mechanical properties of reinforced
composites. The tensile strength (3695.316 MPa) and flexural strength (105.5754Mpa) is highest for inclined orientated
fibers compared to that of Linear & Bi-directional oriented fibers. The Higher impact strength of 3.69 KJ/m2
was
obtained for Bi-directional orientated fibers.
Keywords: Pineapple Leaf Fiber, Bisphenol, Orientation, Tensile Strength, Flexural Strength, Impact Strength.
I. INTRODUCTION
Composites are one of the most advanced and adaptable engineering materials known to men. Progresses in the
field of materials science and technology have given birth to these fascinating and wonderful materials. Composites are
heterogeneous in nature, created by the assembly of two or more components with fillers or reinforcing fibers and a
compactable matrix [1]. The matrix may be metallic, ceramic or polymeric in origin. Based on the types of reinforcement
used, the composites are classified as particulate, laminate and fiber reinforced composites.
Composites made of natural fibers have received increasing attention in light of the growing environmental
awareness. Also because of their low density, good mechanical performance, unlimited availability and problem free
disposal, natural fibers offer a real alternative to the technical reinforcing fibers presently available. Natural fibers can
compete with glass fibres especially with respect to the specific strength and specific stiffness.
Synthetic fibers are the most widely used to reinforce plastics due to their low cost and fairly good mechanical
properties. However, these fibers have serious drawbacks as high density, non-renewability, non-biodegradability, high
energy consumption etc. Growing environmental awareness and societal concern, a high rate of depletion of petroleum
resources, the concept of sustainability, and new environmental regulations have triggered the search for new products
that are compatible with the environment. Sustainability, ‘cradle to grave’ design, industrial ecology, eco-friendly and
bio-compatibility are the guiding principles of development of new generation materials. Lignocellulosic reinforced
composites are the materials of the new paradigm. The use of biodegradable and environment friendly plant-based fibers
in the composites reduces waste disposal problems, environment pollution and ecological concerns.
INTERNATIONAL JOURNAL OF MECHANICAL ENGINEERING
AND TECHNOLOGY (IJMET)
ISSN 0976 – 6340 (Print)
ISSN 0976 – 6359 (Online)
Volume 5, Issue 9, September (2014), pp. 181-188
© IAEME: www.iaeme.com/IJMET.asp
Journal Impact Factor (2014): 7.5377 (Calculated by GISI)
www.jifactor.com
IJMET
© I A E M E
Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
182
Although there are several reports in the literature which discuss the mechanical behavior of natural fiber
reinforced polymer composites. However, very limited work has been done on effect of fiber orientation on mechanical
behavior of PALF reinforced Bisphenol composites. Against this background, the present research work has been
undertaken, with an objective to explore the potential of PALF as a reinforcing material in polymer composites and to
investigate its effect on the mechanical behavior of the resulting composites.
II. MATERIALS AND METHODOLOGY
Pineapple plants are largely grown in tropical America, in the Far-East Asia countries and Africa. Pineapple
leaves from the plantations are being wasted as they are cut after the fruits are harvested before being either composted or
burnt. Additionally, burning of these beneficial agricultural wastes causes environmental pollution. It is in the Philippines
and Taiwan where the pineapple plant is largely used as a source of fiber. India also uses the pineapple plant as a source
of fiber.
Bisphenol-A (BPA) is an organic compound which belongs to the group of diphenyl methane derivatives and
Bisphenol. The chemical formula is (CH3)2 C (C6H4OH) 2. BPA is used to make certain plastics and epoxy resins; it
has been in commercial use since 1957. Table 2.1 shows some of the properties of Bisphenol resin.
Table 2.1: Properties of Bisphenol resin
Tensile strength 30MPa
Tensile modulus 3300 MPa
Elongation at break 2%
Flexure strength 80MPa
Flexure modulus 3100 Mpa
Melting point 156 - 159 0
C
Specific gravity 1.19 - 1.20
Impact strength 2.0-2.2 kJ/m2
Poisson’s ratio 0.37
2.1 Extraction of fibers
The pineapple fiber bundles are separated from the pineapple leaf by hand and sometimes by machines. The
hand separation involves the stripping off of the fiber from the retted leaf. This method is considered to be laborious and
costly and tends to lose a lot of weaker fibres. The use of machines to separate the fiber bundles is slower than the hand
method of extraction but facilitates production processes. The yield of hand separated pineapple fiber bundles is in the
range 2% to 3% dry fiber from about 1 ton of pineapple leaf, that is, 20 kg to 27 kg of dry fiber [2].
Owing to the above factors, biological method is preferred to mechanical and chemical routes for extracting
fibers of good quality from embedding matrix. It is in this context that National Institute of Interdisciplinary Science and
Technology (NIIST), Trivandrum, Kerala devised a clean anaerobic process yields superior quality fibers while
shortening the processing time substantially. Here separation of fibers from their matrices is achieved by enzymatic
cleaving of cementing compounds with in situ microbial growth and enzyme production. The organic residue generated
by the process is converted to methane that can be recovered for fuel.
2.2 Chemical treatment
Alkali treatment leads to the increase in the amount of amorphous cellulose at the expense of crystalline
cellulose. The important modification occurring here is the removal of hydrogen bonding in the network structure.
Modifying natural fibers with alkali treatment has greatly improved the mechanical properties of the resultant composites
by improving the adhesion between fiber and the matrix material.
The following steps were carried out during chemical treatment:
• 5% NaOH solution was prepared using sodium hydroxide pellets and distilled water.
• Pineapple leaf fibers were then dipped in the solution for 1hour.
• After 1 hour fibers were washed with 1% HCl solution to neutralize the fibers.
• Then it is washed with distilled water.
• It was then kept in hot air oven for 3hours at 65-70°C.
2.3 Manufacturing of composite
A polypropylene (PP) mould having dimensions of 150 X 100 X 4 mm is used for composite fabrication. The
mould was first cleaned with wax so that the laminate easily comes out of the die after hardening. Then around 15 to 20
ml of promoter and accelerator are added to Bisphenol and the color of the resin changes from pale yellow to dark yellow
Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
183
with the addition of these two agents. The laminates of three different fibers orientations mats of unidirectional,
bidirectional and inclined are prepared using hand layup method. This method of manufacturing is a relatively simple
method compared to other methods like vacuum bag molding, resin transfer molding, autoclave molding etc.
Figure 2.1. Laminates with fibers in Uni-direction, Bi-direction and Inclined
Figure 2.1shows the uni-directional, bi-directional and inclained orinted PALF leaf fiber composites.
III. RESULTS AND DISCUSSION
Orientation of fibers related to one another plays avital role in the performance of composite. The prepared
specimens are cutted according to their specific ASTM standards and analysed. The tensile, flexural and impact test was
carriedout for all the laminates of three different fibers mats of unidirectional, bidirectional and inclined orientations.
i) Tensile test: The tensile test were conducted following the standard of ASTM D638 (115*19*4mm) is type IV using
JJ Lloyd universal testing machine with load cell of 1kN and using crosshead speed of 5 mm/min. The test was
performed until the tensile failure occurred.
Figure 3.1: Specimen undergoing tensile test
Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
184
Figure3.1(a): Stress-strain curve of Uni-directional Figure 3.1(b):. Stress-strain curve of Bi- directional
composites composites
Figure 3.1(c): Stress-strain curve of inclined PALF composite
Table 3.1: Tensile Test Results
Fiber Orientation Maximum load(kN) Young’s Modulus(MPa) Stress at maximum load (MPa)
Uni-directional 1.182531145 3156.926454 37.18522358
Bi-directional 0.892445366 3508.677367 49.27213103
Inclined 1.199897217 3695.316033 49.99571739
Figure 3.1 a, b, c shows the Stress-strain curve of Uni, Bi and Inclined direction PALF composite. From table
3.1 it can be seen that the highest Young’s modulus is 3695.31Mpa for inclined orientated fibers which is 10.69% greater
than the matrix material Bisphenol. Initially for Uni-directionally orientated fiber’s Young’s modulus value 4.33% lesser
than the matrix material. But when the orientation of the fiber changes to bi-directional Young’s modulus increased by
5.49% with respect to that of matrix material.
ii) Flexural Test: Flexural strength, also known as modulus of rupture, bend strength, or fracture strength. The flexural
strength represents the highest stress experienced within the material at its moment of rupture. There are two methods
that cover the determination of flexural properties of material: three-point loading system and four point loading system.
Here ASTM D790 (125*14.5*4mm), three-point loading system applied on a supported beam was utilized. The flexural
test was conducted using JJ Lloyd universal testing machine with load cell of 1kN and using crosshead speed of 5
mm/min. The test was performed until the flexural failure occurred.
Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
185
Figure 3.2: Specimen undergoing flexural test
Figure3.2(a): Stress- Bending strain curve of Uni-directional and Bi-directional composites
Figure3.2(b): Stress- Bending strain curve of inclined composites
Figure 3.2 a, b shows the Stress-strain curve of Uni, Bi and Inclined direction PALF composite. From table 3.2
it can be seen that the highest value of maximum bending stress is 105.57Mpa for inclined orientated fibers which is
24.22% greater than the matrix material Bisphenol. Initially for Uni-directionally orientated fibers maximum bending
stress drastically increased by 4.3% and for bi-directional orientated fibers it is increased to 22.21% than the matrix
material. Hence fiber orientation greatly inlfuences the flexural property of the material where load carrying ability of the
fibers changes with respect to its orientation.
Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
186
Table 3.2: Flexural test results
Fiber Orientation Maximum load(KN) Maximum bending stress (MPa)
Uni-directional 0.226514998 83.60543723
Bi-directional 0.278678076 102.8585419
Inclined 0.286039163 105.5754786
Figure 3.2(c): Variation of Maximum bending stress with fiber orientation
Figure 3.2(c) shows the graph of maximum bending stress v/s fiber length. For Uni-directionally orientated
fibers the value is 83.60Mpa and it increased by 18.71% when the fiber orientation changes to bi-directional. Further the
value increased by 2.57% when the fiber orientation changes from bi-directional to incline.
iii) Impact test: Impact strength is also known as the ability of the material to absorb mechanical energy in the process
of deformation and fracture under impact loading. The impact properties of the unidirectional, bidirectional and inclined
PALF reinforced composites was studied. Charpy impact test was carried out on a test specimen as per (ASTM D256-
(65*14.5mm)).
Figure 3.3: Test Specimen undergoing impact test
The table 3.1 shows that the highest value of Charpy impact strength is 3.69kJ/m2
for Bi-directional oriented
fiber which is 45.79% greater than the matrix material Bisphenol. InitiallyUni-directionally orientated fibers impact
strength increased by 37.5%.Then its value slightly increased by 18.69% forinclined orientated fibers.
Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
187
Table 3.3: Impact test results
Fiber Orientation Charpy impact strength (kJ/m2
)
Uni-directional 3.2
Bi-directional 3.69
Inclined 2.46
Figure 3.3(a): Variation of Charpy impact strength with fiber length
Figure 3.3(a) shows Charpy impact strength V/s Fiber orientation. For Uni-directionally orientated fibers the
Charpy impact strength is 3.2 kJ/m2
and it increased by 13.27% when the fiber orientation changes to bi-directional.
Further the value decreased by 33% when the fiber orientation changes from bi-directional to incline. It is generally
accepted that the toughness of a fiber composite is mainly dependent on the fiber stress-strain behavior especially the
strong fibers such as PALF with high failure strain which can actually impart high work to fracture on the composites.
IV. CONCLUSION
The results of this present study showed that a useful composite with good properties could be successfully
developed using treated PALF as reinforcing agent for the Bisphenol matrix. It can be seen that inclined oriented
composites show better tensile strength of 49.9957MPa than Uni-directional and bi-directional oriented composites.
inclined oriented composites show better flexural strength of 105.57 MPa than Uni-directional and bi-directional oriented
composites. impact strength of 3.69 KJ/m2
Bi-directional oriented composites show better impact strength than Uni-
directional and inclained oriented composites. Hence fiber orientation greatly influence the mechanical properties of the
PALF reinforced Bisphenol composite.
V. REFERENCES
[1] Lubin , Hand book of composites, Van Nostarnd, New York, 1982.
[2] Kirby, R. H. Vegetable Fibres, Interscience Publishers, New York, 1963, Chapter xvi.
[3] Drzal, L.T., Mohanty, A.K., Burgueño, R. and Misra, M. (2003). Biobased Structural Composite Materials for
Housing and Infrastructure Applications: Opportunities and Challenges. Composite Science and Technology.
63: 129-140.
[4] Shackelford, J.F. (1992). Introduction to Materials Science for Engineers. 4th ed.United Kingdom: Prentice-
Hall, Inc. 153-159.
[5] Ramakrishna Malkapuram, Vivek Kumar, and Yuvraj Singh NegiRecent Development in Natural Fiber
Reinforced Polypropylene Composites Journal of Reinforced Plastics and Composites 2009
28:1169-1189:10.1177/0731684407087759.
[6] Processing and characterization of natural fiber reinforced polymer composites, a thesis submitted by
PrakashTudu, NIT Rourkela.
[7] Arib, R.M.N., Sapuan, S.M., Hamdan, M.A.M.M., Paridah, M.T. and Zaman, H.M.D.K. (2004). A Literature
Review of Pineapple Fiber Reinforced Polymer Composites. Polymer and Polymer Composites.
12(4): 341-348.
[8] Munirahmokhtar, Abdul Rrazakrahmat, Azman Hassan (2007) Characterization and treatments of pineapple
leaf fiber thermoplastic composite for construction applications volume 75147.
Proceedings of the 2nd
International Conference on Current Trends in Engineering and Management ICCTEM -2014
17 – 19, July 2014, Mysore, Karnataka, India
188
[9] Uma Devi, L., Bhagawan, S.S. and Thomas, S. (1997). Mechanical Properties of Pineapple Leaf Fiber-
Reinforced Polyester Composites. Journal of Applied Polymer Science. 64: 1739-1748.
[10] American Standard of Testing and Materials-ASTM International (2003). Standard Test Method for Tensile
Properties of Plastics. United State, ASTM 638-03.
[11] American Standard of Testing and Materials-ASTM International (2003). Standard Test Methods for Flexural
Properties of Unreinforced and Reinforced Plasticsand Electrical Insulating Materials. United State, ASTM
D790-03.
[12] Arib, R.M.N. (2003). Mechanical Properties of Pineapple Leaf Fiber Reinforced Polypropylene Laminated
Composites. University Putra Malaysia. Master’s Thesis.

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STUDY ON THE INFLUENCE OF FIBER ORIENTATION ON PALF REINFORCED BISPHENOL COMPOSITES

  • 1. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 181 STUDY ON THE INFLUENCE OF FIBER ORIENTATION ON PALF REINFORCED BISPHENOL COMPOSITES Vinod B1 , Dr. Sudev L J2 1 Asst Professor, Department of Mechanical Engg, VVCE, Mysore, India 2 Professor, Department of Mechanical Engg, VVCE, Mysore, India ABSTRACT The main advantage of a composite material over conventional material like a monolithic metal is the combination of different properties which are seldom found in the conventional material. In recent years natural fibers appear to be the outstanding materials which come as the viable and abundant substitute for the expensive and nonrenewable synthetic fiber. Pineapple leaf fiber (PALF) is one of them that have also good potential as reinforcement in thermoset composite. The objective of the present work is to investigate the effect of fiber orientation on the mechanical properties of PALF reinforced Bisphenol composite and explores the potential of using PALF as reinforcing material. In this paper the mechanical properties like tensile, flexural and impact behavior are studied. From this experimental study, it was observed that the fiber orientation greatly influences the mechanical properties of reinforced composites. The tensile strength (3695.316 MPa) and flexural strength (105.5754Mpa) is highest for inclined orientated fibers compared to that of Linear & Bi-directional oriented fibers. The Higher impact strength of 3.69 KJ/m2 was obtained for Bi-directional orientated fibers. Keywords: Pineapple Leaf Fiber, Bisphenol, Orientation, Tensile Strength, Flexural Strength, Impact Strength. I. INTRODUCTION Composites are one of the most advanced and adaptable engineering materials known to men. Progresses in the field of materials science and technology have given birth to these fascinating and wonderful materials. Composites are heterogeneous in nature, created by the assembly of two or more components with fillers or reinforcing fibers and a compactable matrix [1]. The matrix may be metallic, ceramic or polymeric in origin. Based on the types of reinforcement used, the composites are classified as particulate, laminate and fiber reinforced composites. Composites made of natural fibers have received increasing attention in light of the growing environmental awareness. Also because of their low density, good mechanical performance, unlimited availability and problem free disposal, natural fibers offer a real alternative to the technical reinforcing fibers presently available. Natural fibers can compete with glass fibres especially with respect to the specific strength and specific stiffness. Synthetic fibers are the most widely used to reinforce plastics due to their low cost and fairly good mechanical properties. However, these fibers have serious drawbacks as high density, non-renewability, non-biodegradability, high energy consumption etc. Growing environmental awareness and societal concern, a high rate of depletion of petroleum resources, the concept of sustainability, and new environmental regulations have triggered the search for new products that are compatible with the environment. Sustainability, ‘cradle to grave’ design, industrial ecology, eco-friendly and bio-compatibility are the guiding principles of development of new generation materials. Lignocellulosic reinforced composites are the materials of the new paradigm. The use of biodegradable and environment friendly plant-based fibers in the composites reduces waste disposal problems, environment pollution and ecological concerns. INTERNATIONAL JOURNAL OF MECHANICAL ENGINEERING AND TECHNOLOGY (IJMET) ISSN 0976 – 6340 (Print) ISSN 0976 – 6359 (Online) Volume 5, Issue 9, September (2014), pp. 181-188 © IAEME: www.iaeme.com/IJMET.asp Journal Impact Factor (2014): 7.5377 (Calculated by GISI) www.jifactor.com IJMET © I A E M E
  • 2. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 182 Although there are several reports in the literature which discuss the mechanical behavior of natural fiber reinforced polymer composites. However, very limited work has been done on effect of fiber orientation on mechanical behavior of PALF reinforced Bisphenol composites. Against this background, the present research work has been undertaken, with an objective to explore the potential of PALF as a reinforcing material in polymer composites and to investigate its effect on the mechanical behavior of the resulting composites. II. MATERIALS AND METHODOLOGY Pineapple plants are largely grown in tropical America, in the Far-East Asia countries and Africa. Pineapple leaves from the plantations are being wasted as they are cut after the fruits are harvested before being either composted or burnt. Additionally, burning of these beneficial agricultural wastes causes environmental pollution. It is in the Philippines and Taiwan where the pineapple plant is largely used as a source of fiber. India also uses the pineapple plant as a source of fiber. Bisphenol-A (BPA) is an organic compound which belongs to the group of diphenyl methane derivatives and Bisphenol. The chemical formula is (CH3)2 C (C6H4OH) 2. BPA is used to make certain plastics and epoxy resins; it has been in commercial use since 1957. Table 2.1 shows some of the properties of Bisphenol resin. Table 2.1: Properties of Bisphenol resin Tensile strength 30MPa Tensile modulus 3300 MPa Elongation at break 2% Flexure strength 80MPa Flexure modulus 3100 Mpa Melting point 156 - 159 0 C Specific gravity 1.19 - 1.20 Impact strength 2.0-2.2 kJ/m2 Poisson’s ratio 0.37 2.1 Extraction of fibers The pineapple fiber bundles are separated from the pineapple leaf by hand and sometimes by machines. The hand separation involves the stripping off of the fiber from the retted leaf. This method is considered to be laborious and costly and tends to lose a lot of weaker fibres. The use of machines to separate the fiber bundles is slower than the hand method of extraction but facilitates production processes. The yield of hand separated pineapple fiber bundles is in the range 2% to 3% dry fiber from about 1 ton of pineapple leaf, that is, 20 kg to 27 kg of dry fiber [2]. Owing to the above factors, biological method is preferred to mechanical and chemical routes for extracting fibers of good quality from embedding matrix. It is in this context that National Institute of Interdisciplinary Science and Technology (NIIST), Trivandrum, Kerala devised a clean anaerobic process yields superior quality fibers while shortening the processing time substantially. Here separation of fibers from their matrices is achieved by enzymatic cleaving of cementing compounds with in situ microbial growth and enzyme production. The organic residue generated by the process is converted to methane that can be recovered for fuel. 2.2 Chemical treatment Alkali treatment leads to the increase in the amount of amorphous cellulose at the expense of crystalline cellulose. The important modification occurring here is the removal of hydrogen bonding in the network structure. Modifying natural fibers with alkali treatment has greatly improved the mechanical properties of the resultant composites by improving the adhesion between fiber and the matrix material. The following steps were carried out during chemical treatment: • 5% NaOH solution was prepared using sodium hydroxide pellets and distilled water. • Pineapple leaf fibers were then dipped in the solution for 1hour. • After 1 hour fibers were washed with 1% HCl solution to neutralize the fibers. • Then it is washed with distilled water. • It was then kept in hot air oven for 3hours at 65-70°C. 2.3 Manufacturing of composite A polypropylene (PP) mould having dimensions of 150 X 100 X 4 mm is used for composite fabrication. The mould was first cleaned with wax so that the laminate easily comes out of the die after hardening. Then around 15 to 20 ml of promoter and accelerator are added to Bisphenol and the color of the resin changes from pale yellow to dark yellow
  • 3. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 183 with the addition of these two agents. The laminates of three different fibers orientations mats of unidirectional, bidirectional and inclined are prepared using hand layup method. This method of manufacturing is a relatively simple method compared to other methods like vacuum bag molding, resin transfer molding, autoclave molding etc. Figure 2.1. Laminates with fibers in Uni-direction, Bi-direction and Inclined Figure 2.1shows the uni-directional, bi-directional and inclained orinted PALF leaf fiber composites. III. RESULTS AND DISCUSSION Orientation of fibers related to one another plays avital role in the performance of composite. The prepared specimens are cutted according to their specific ASTM standards and analysed. The tensile, flexural and impact test was carriedout for all the laminates of three different fibers mats of unidirectional, bidirectional and inclined orientations. i) Tensile test: The tensile test were conducted following the standard of ASTM D638 (115*19*4mm) is type IV using JJ Lloyd universal testing machine with load cell of 1kN and using crosshead speed of 5 mm/min. The test was performed until the tensile failure occurred. Figure 3.1: Specimen undergoing tensile test
  • 4. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 184 Figure3.1(a): Stress-strain curve of Uni-directional Figure 3.1(b):. Stress-strain curve of Bi- directional composites composites Figure 3.1(c): Stress-strain curve of inclined PALF composite Table 3.1: Tensile Test Results Fiber Orientation Maximum load(kN) Young’s Modulus(MPa) Stress at maximum load (MPa) Uni-directional 1.182531145 3156.926454 37.18522358 Bi-directional 0.892445366 3508.677367 49.27213103 Inclined 1.199897217 3695.316033 49.99571739 Figure 3.1 a, b, c shows the Stress-strain curve of Uni, Bi and Inclined direction PALF composite. From table 3.1 it can be seen that the highest Young’s modulus is 3695.31Mpa for inclined orientated fibers which is 10.69% greater than the matrix material Bisphenol. Initially for Uni-directionally orientated fiber’s Young’s modulus value 4.33% lesser than the matrix material. But when the orientation of the fiber changes to bi-directional Young’s modulus increased by 5.49% with respect to that of matrix material. ii) Flexural Test: Flexural strength, also known as modulus of rupture, bend strength, or fracture strength. The flexural strength represents the highest stress experienced within the material at its moment of rupture. There are two methods that cover the determination of flexural properties of material: three-point loading system and four point loading system. Here ASTM D790 (125*14.5*4mm), three-point loading system applied on a supported beam was utilized. The flexural test was conducted using JJ Lloyd universal testing machine with load cell of 1kN and using crosshead speed of 5 mm/min. The test was performed until the flexural failure occurred.
  • 5. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 185 Figure 3.2: Specimen undergoing flexural test Figure3.2(a): Stress- Bending strain curve of Uni-directional and Bi-directional composites Figure3.2(b): Stress- Bending strain curve of inclined composites Figure 3.2 a, b shows the Stress-strain curve of Uni, Bi and Inclined direction PALF composite. From table 3.2 it can be seen that the highest value of maximum bending stress is 105.57Mpa for inclined orientated fibers which is 24.22% greater than the matrix material Bisphenol. Initially for Uni-directionally orientated fibers maximum bending stress drastically increased by 4.3% and for bi-directional orientated fibers it is increased to 22.21% than the matrix material. Hence fiber orientation greatly inlfuences the flexural property of the material where load carrying ability of the fibers changes with respect to its orientation.
  • 6. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 186 Table 3.2: Flexural test results Fiber Orientation Maximum load(KN) Maximum bending stress (MPa) Uni-directional 0.226514998 83.60543723 Bi-directional 0.278678076 102.8585419 Inclined 0.286039163 105.5754786 Figure 3.2(c): Variation of Maximum bending stress with fiber orientation Figure 3.2(c) shows the graph of maximum bending stress v/s fiber length. For Uni-directionally orientated fibers the value is 83.60Mpa and it increased by 18.71% when the fiber orientation changes to bi-directional. Further the value increased by 2.57% when the fiber orientation changes from bi-directional to incline. iii) Impact test: Impact strength is also known as the ability of the material to absorb mechanical energy in the process of deformation and fracture under impact loading. The impact properties of the unidirectional, bidirectional and inclined PALF reinforced composites was studied. Charpy impact test was carried out on a test specimen as per (ASTM D256- (65*14.5mm)). Figure 3.3: Test Specimen undergoing impact test The table 3.1 shows that the highest value of Charpy impact strength is 3.69kJ/m2 for Bi-directional oriented fiber which is 45.79% greater than the matrix material Bisphenol. InitiallyUni-directionally orientated fibers impact strength increased by 37.5%.Then its value slightly increased by 18.69% forinclined orientated fibers.
  • 7. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 187 Table 3.3: Impact test results Fiber Orientation Charpy impact strength (kJ/m2 ) Uni-directional 3.2 Bi-directional 3.69 Inclined 2.46 Figure 3.3(a): Variation of Charpy impact strength with fiber length Figure 3.3(a) shows Charpy impact strength V/s Fiber orientation. For Uni-directionally orientated fibers the Charpy impact strength is 3.2 kJ/m2 and it increased by 13.27% when the fiber orientation changes to bi-directional. Further the value decreased by 33% when the fiber orientation changes from bi-directional to incline. It is generally accepted that the toughness of a fiber composite is mainly dependent on the fiber stress-strain behavior especially the strong fibers such as PALF with high failure strain which can actually impart high work to fracture on the composites. IV. CONCLUSION The results of this present study showed that a useful composite with good properties could be successfully developed using treated PALF as reinforcing agent for the Bisphenol matrix. It can be seen that inclined oriented composites show better tensile strength of 49.9957MPa than Uni-directional and bi-directional oriented composites. inclined oriented composites show better flexural strength of 105.57 MPa than Uni-directional and bi-directional oriented composites. impact strength of 3.69 KJ/m2 Bi-directional oriented composites show better impact strength than Uni- directional and inclained oriented composites. Hence fiber orientation greatly influence the mechanical properties of the PALF reinforced Bisphenol composite. V. REFERENCES [1] Lubin , Hand book of composites, Van Nostarnd, New York, 1982. [2] Kirby, R. H. Vegetable Fibres, Interscience Publishers, New York, 1963, Chapter xvi. [3] Drzal, L.T., Mohanty, A.K., Burgueño, R. and Misra, M. (2003). Biobased Structural Composite Materials for Housing and Infrastructure Applications: Opportunities and Challenges. Composite Science and Technology. 63: 129-140. [4] Shackelford, J.F. (1992). Introduction to Materials Science for Engineers. 4th ed.United Kingdom: Prentice- Hall, Inc. 153-159. [5] Ramakrishna Malkapuram, Vivek Kumar, and Yuvraj Singh NegiRecent Development in Natural Fiber Reinforced Polypropylene Composites Journal of Reinforced Plastics and Composites 2009 28:1169-1189:10.1177/0731684407087759. [6] Processing and characterization of natural fiber reinforced polymer composites, a thesis submitted by PrakashTudu, NIT Rourkela. [7] Arib, R.M.N., Sapuan, S.M., Hamdan, M.A.M.M., Paridah, M.T. and Zaman, H.M.D.K. (2004). A Literature Review of Pineapple Fiber Reinforced Polymer Composites. Polymer and Polymer Composites. 12(4): 341-348. [8] Munirahmokhtar, Abdul Rrazakrahmat, Azman Hassan (2007) Characterization and treatments of pineapple leaf fiber thermoplastic composite for construction applications volume 75147.
  • 8. Proceedings of the 2nd International Conference on Current Trends in Engineering and Management ICCTEM -2014 17 – 19, July 2014, Mysore, Karnataka, India 188 [9] Uma Devi, L., Bhagawan, S.S. and Thomas, S. (1997). Mechanical Properties of Pineapple Leaf Fiber- Reinforced Polyester Composites. Journal of Applied Polymer Science. 64: 1739-1748. [10] American Standard of Testing and Materials-ASTM International (2003). Standard Test Method for Tensile Properties of Plastics. United State, ASTM 638-03. [11] American Standard of Testing and Materials-ASTM International (2003). Standard Test Methods for Flexural Properties of Unreinforced and Reinforced Plasticsand Electrical Insulating Materials. United State, ASTM D790-03. [12] Arib, R.M.N. (2003). Mechanical Properties of Pineapple Leaf Fiber Reinforced Polypropylene Laminated Composites. University Putra Malaysia. Master’s Thesis.
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